By Paul J. Eslinger PhD
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Extra resources for Neuropsychological interventions : clinical research and practice
Single-Wavelength Attenuated Total Reﬂection–Based Devices Wilks Enterprises (South Norwalk, MA)  recently introduced a device incorporating a miniature attenuated total reﬂection (ATR) cell as its interface. The device resembles an old-fashioned electrical fuse for a home fuse box. In place of the metal contact at the base, a small ATR cell protrudes from the base. Through this, monochromatic light courses. The light is produced by a small, single-wavelength source within the housing and detected by a small detector alongside it.
Small standard deviations indicate homogenous blends, whereas larger standard deviations indicate less homogeneity. An F test or chi-square test of the variance, depending on the sampling protocol, allows determination of homogeneity at the desired conﬁdence level. Williams  has commented on the standard deviation as a measure of quality for a mixture of dry powders. The technique offers certain disadvantages, according to Williams. First, a pharmaceutical mixture is a complex assembly of particles and it may not be reasonable to assume that it can be adequately described by a single statistic like standard deviation.
Although the standard deviations drop to a minimum at the point which homoCopyright 2002 by Marcel Dekker, Inc. All Rights Reserved geneity is reached, as seen in plots of standard deviation versus time, no statistical test was suggested for the identiﬁcation of homogeneity with any particular degree of certainty. In three experiments conducted by Aldridge et al. the spectral data showed the blend to be homogenous before a typical blending period of about 15 to 20 min is complete. Wargo and Drennen discussed their near-IR characterization of pharmaceutical powder blends in a 1996 paper .
Neuropsychological interventions : clinical research and practice by Paul J. Eslinger PhD